<p>Mortar
samples were prepared with sulphide-bearing aggregates and tested for the
potential of aggregate oxidation and its subsequent sulphate attack. Scanning
Electron Microscopy (SEM) was used as a tool to analyze the developed phases in
the samples to confirm that the obtained expansion is attributable to sulphate
attack. The Energy Dispersive X-Ray analysis (EDS) of the SEM helped to
identify sulphide phases in aggregates and the presence of evidence of sulphate
attack in mortars exposed to conditions that promote oxidation and sulphate
attack. Ettringite and Thaumasite were detected and confirmed by EDS in the
mortars with sulphide-bearing aggregates suggesting that the test conditions
are suitable for reproducing the damaging mechanism of sulphide
oxidation. </p><p><br></p><p>Elmosallamy, Monaand Shehata, Medhat H.Microscopic analysis for the oxidation of sulphide-bearing aggregate, Journalof Microscopy, SN -0022-2720, https://doi.org/10.1111/jmi.13065<br></p>